Abstract: Synthesis of 1,3,5-tris(2-aryloxyethyl)isocyanurates by esterification of 1,3,5-tris(2-hydroxyethyl)isocyanurate under microwave irradiation in a direct and efficient way in solvent free conditions.

Abstract: Microwave assisted synthesis of 1,3,5-tris(2-hydroxyethyl)isocyanurate carbamates under solventless conditions in short times and good yields is described.

Abstract: Novel quinoline derivatives was designed as anticancer iron chelators. Structurally they combine active moieties of known quinoline and thiosemicarbazone bioeffectors. For the synthetic part of study we applied microvawe assisted techniques MAOS. Resulted compounds exhibited interesting anticancer activities against HCT116 cancer cells.

Abstract: In this work, vegetable polyols as a potential replacement of petroleum polyols were investigated. The two-stage method of preparation natural oil-derived polyols was presented.

Abstract: The title compound, [6-Diethylamino-9-(2-octylcarbamoyl-phenyl)-xanthen-3-ylidene]-diethyl-amine was synthesized in high yield by an amidation with N-octylamine in a CEM Discover microwave at 60°C for 2 hrs. Its structure was characterized by Ultraviolet-Visible and fluorescence spectral analysis.

Abstract: Copper sulfide nanoparticles were synthesized by microwave irradiation, by the decomposition of [Cu(NH₂CSNH₂)₂]Cl₂ complex, formed by the reaction of copper(II) acetate, thiourea (Tu) in the presence of surfactant Sodium dodecyl sulfate (SDS). X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared (FT-IR) used to characterize the product. The result nanoparticles have a diameter of about 60-70 nm.

Abstract: 1,2,4,5-Benzenetetracarboxylic acid (H4btec) with transition metal ions Co(II) and Ni (II), give two coordination complexes, C₁₀H₁₆CoO₁₄ (I) and C₁₀H₁₈Na₂NiO₁₆ (II). These complexes have been synthesized by a fast and efficient method under microwave irradiation. These compounds have been characterized by FT-IR spectroscopy and elemental analysis.

Abstract: Reaction of substituted acetophenone (hepta-O-acetyl-b-maltosyl)thiosemicarbazones with ethyl bromoacetate was investigated. It's indicated that the nature of solvents and the catalysts affected the reaction yields, and that the microwave-assisted heating method gave higher yields of products than the conventional heating one.

Abstract: Reaction of substituted acetophenone (hepta-O-acetyl-b-lactosyl)thiosemicarbazones with ethyl bromoacetate was performed in the presence of anhydrous sodium acetate using microwave-assisted heating method. The reaction yields were 64-80%. Structure of 2-iminothiazolidin-4-one products was confirmed by spectroscopic methods. Isomer ratios 2 and 2' were determined by ¹H NMR.

Abstract: A series of substituted benzaldehyde hepta-O-acetyl-b-lactosyl thiosemicarbazones were synthesized by condensation reactions of hepta-O-acetyl-b-lactosyl thiosemicarbazide with corresponding substituted benzaldehydes. Structures of thiosemicarbazones were confirmed by spectroscopic (IR, NMR) methods. The ¹H and ¹³C NMR spectra of substituted acetophenone peracetylated b-lactosyl thiosemicarbazones have been recorded and discussed. The magnetic resonance signals in their NMR spectra show the relationships between the structure and positions of the substituted groups by Hammett's regression. The b anomeric configuration of these thiosemicarbazones was confirmed on the basis of the coupling constant J = 9.5–8.5 Hz between proton NH-4 of thiosemicarbazone bond and proton H-1' in lactosyl component

Abstract: A novel rapid one-pot four-component reaction between resorcinol, aromatic aldehydes, malononitrile and ammonium acetate in aqueous media was performed under microwave irradiation for the synthesis of 1,4-dihydroquinoline derivatives. The main advantages of this method are the short reaction time, high yields, despite absence of any catalyst, and simple work-up.

Abstract: A series of per-O-acetyl-b-D-glycosyl thiosemicarbazones 4 and 5 of benzaldehydes and acetophenones were obtained from reaction of per-O-acetyl-b-maltosyl thiosemicarbazide 1 with corresponding carbonyl compounds (2 and 3) in ethanol or acetic acid as solvent using microwave-assisted method. The positions of the magnetic resonance signals in their NMR spectra and the substituent's nature have been indicated by Hammett's regression. The b anomeric configuration of these thiosemicarbazones was confirmed on the basis of the coupling constant J = 9.0–9.5 Hz between proton NH-4 of thiosemicarbazone bond and proton H-1' in maltose component. Structures of thiosemicarbazones were confirmed by spectroscopic methods

Abstract: 5H-Pyrido[4,3-b]indole was obtained from 3-formylindole in 16% overall yield by Jackson and Shannon modification of the Pomeranz-Fristch isoquinoline synthesis. The final cyclisation occurred but the removal of the tosyl group and oxidation of the dihydrocompound was not efficient. Changes in the concentration of the acid catalyst gave 29% as the best yield for the last step. An NMR study of the cyclisation is described.

Abstract: In this paper microwave-assisted synthesis of a special catalyst, namely, Pt/C catalyst comprised of nanoparticles is discussed. Owing to its unique characteristics, the catalyst is very beneficial to the performance of proton exchange membrane fuel cells (PEMFCs). As mentioned in the article, Pt nanoparticles once integrated with Carbon, provide better catalytic activity/stability. Such integration has been achieved successfully by microwave heating. The relevant experimental works of some researchers are briefly reviewed in the end.