Cite this paper as: Vázquez- Fernández, M.; Fernández-García, M.; Fernández, B.; Gonzalez-Noya, A.; Maneiro, M.; Rodríguez-Doutón, M. CRYSTAL STRUCTURE OF (N-N'-BIS(3-ETHOXYSALICYLIDENE)-1,2-DIAMINOPROPANE. In Proceedings of the 13th Int. Electron. Conf. Synth. Org. Chem., 1-30 November 2009; Sciforum Electronic Conferences Series, 2009, a023:1-3.
13th Int. Electron. Conf. Synth. Org. Chem. 2009, a023:1-3
Communication
CRYSTAL STRUCTURE OF (N-N'-BIS(3-ETHOXYSALICYLIDENE)-1,2-DIAMINOPROPANE
Dpto. de Química Inorgánica. Facultad de Ciencias. Univ. de Santiago de Compostela, Lugo 27002, Spain;
* Author to whom correspondence should be addressed.
(This article belongs to the section A. General Organic Synthesis)
Abstract: Three hexadentate Schiff base ligands were obtained by condensation of 3-ethoxy-2-hydroxybenzaldehyde and different diamines (1,2-diaminoethane, 1,2-diaminopropane, 1,2-diamino-2-metylpropane) to yield H2Ln (H2L1, H2L2 and H2L3, respectively). The ligands have been characterised by elemental analysis, IR, and 1H and 13C NMR spectroscopic techniques, mass spectrometry (ES) and X-ray diffraction.
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