Solvent-free synthesis of Thiocarbamic acid [(furan-2-yl) ethylidene] hydrazide under ball-milling conditions

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ECSOC-13 | General Organic Synthesis

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13th Int. Electron. Conf. Synth. Org. Chem. 2009, a026:1-3

Communication

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Solvent-free synthesis of Thiocarbamic acid [(furan-2-yl) ethylidene] hydrazide under ball-milling conditions

Azadeh Tadjarodi*

and Saeedeh Eslami Nezhad

Chemistry Faculty, Iran University of Science and Technology, Narmak, Tehran, Iran; * Author to whom correspondence should be addressed.

(This article belongs to the section A. General Organic Synthesis)

Cite this paper as: Tadjarodi, A.; Nezhad, S. Solvent-free synthesis of Thiocarbamic acid [(furan-2-yl) ethylidene] hydrazide under ball-milling conditions. In Proceedings of the 13th Int. Electron. Conf. Synth. Org. Chem., 1-30 November 2009; Sciforum Electronic Conferences Series, 2009, a026:1-3.

Abstract: Thiocarbamic acid [(furan-2-yl) ethylidene] hydrazide has been synthesized by the reaction between 2-acetylfuran and thiosemicarbazide in 1:1 molar ratio under ball milling conditions. The title compound has been characterized by FT-IR and elemental analysis.

Keywords: Solvent free; Thiosemicarbazide; 2-acetyl furan; Ball milling

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